Experimental investigation of water sensitivity effects on microscale
mechanical behavior of shale
Abstract
Drilling and multi-stage hydraulic fracturing bring a large amount of
water into the formation, and clay-bearing shale reservoirs interact
with water, which may lead to reduction of gas production, attenuation
of fracturing effects, and even wellbore instability. Because of the
complex fabric of shale, a thorough understanding of changes in shale
micromechanics and corresponding mechanisms when exposed to water
remains unclear. In this work, representative terrestrial and marine
shale samples were selected for experiments based on clay enrichment.
Then, contact resonance (CR) technique was performed to characterize
micromechanics of shale after exposure to water. Visual phenomena
provided by environmental scanning electron microscopy (ESEM) assisted
to explain the underlying mechanisms. It was found that the hydration
effect lowered both the storage modulus and stiffness of samples, but
with different contributions from brittle minerals and clay, as well as
variations depending on bedding plane orientation. Owing to the
difference in composition, terrestrial shale exhibited stronger water
sensitivity and anisotropy, with a general 15%-25% decrease in
modulus, while marine shale changed relatively little (-5%-15%).
Moreover, microscopic observation experiments revealed that complex
interaction mechanisms may have existed that produced the mechanical
changes. The reduction of capillary force and the interlaminar swelling
of clay particles after water adsorption weakened the strength-related
behavior of shale. However, the swelling-caused confining effect or void
space closure during the water imbibition process might have offset this
weakening effect, and even increased mechanical properties. At
mesoscale, excessive shrinkage caused the growth of micro-cracks, which
significantly attenuated overall mechanical behavior.